One step protocol and green synthesis of 2-N,N-dimethylamino-3-alkyl(aryl)-2-oxido-1- hydro-2-benzo[1,3,2]diazaphosphinine-4-one derivatives
نویسندگان
چکیده
ABSTRACT. 2-N,N-dimethylamino-2-oxido-3-alkyl(aryl)-1-hydro-2-benzo[1,3,2]diazaphosphinin-4-one (2) derivatives are synthesized by one pot reaction reacting equimolar quantities of anthranilic acid, primary amine, and N,N-dimethylphosphoramic dichloride under reflux ethanol with good yields. The structure the compounds were established on basis their infrared, nuclear magnetic resonance spectral data (1H NMR, 13C NMR 31P NMR), mass spectrometry, elemental analysis.
 
 KEY WORDS: Anthranilic N,N-Dimethylphosphoramic dichloride, Diazaphosphinine
 Bull. Chem. Soc. Ethiop. 2022, 36(4), 859-864. DOI: https://dx.doi.org/10.4314/bcse.v36i4.11
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ژورنال
عنوان ژورنال: Bulletin of The Chemical Society of Ethiopia
سال: 2022
ISSN: ['1011-3924', '1726-801X']
DOI: https://doi.org/10.4314/bcse.v36i4.11